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ACTA Pharmaceutica Sciencia
2004 , Vol 46 , Num 1
LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY ANALYSIS OF HIGH MOLECULAR WEIGHT AZINES
Department of Chemistry Faculty of Science Mu'tah University Al-Karak, Jordan
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(+)- Electrospray mass spectrometry ionization interlace is a powerful tool in determining molecular weight of large, non-volatile or polar organic compounds. Mass analysis of three different azine derivatives 1-3, recently prepared in our lab., was conducted using LCDuo ion-trap quadruple LC-MS equipped with (+) - electrospray ionization interface. Molecular ions observed were [M]+, [MH]+ as well as dimers, sodium and potassium adduct ions for the three compounds.
Keywords :
LC- MS,BICYCLIC AZINE N ALLYL PYRAZOLE, TETRAENE AZINE